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Molecular Vista “Vista 300” PiF microscope
Industry-leading automation
This instrument allows access to features on samples as large as 300 mm with PiFM & PiF-IR.
AutoPiFM and AutoAlign make Vista 300 the most advanced nano IR instrument ever made.
With sub-5 nm IR spatial resolution and single-molecule-level sensitivity, Vista 300 can help you efficiently solve tough problems in research, failure analysis, or fabrication facilities.
Vista 300 is the most advanced nano-chemical meteorology instrument for R&D and failure analysis in nanofabrication.
Features
AutoPiFM
AutoPiFM generates a complete dataset from scratch, including fixed-wavenumber PiFM images of every chemical component detected, and PiF‑IR spectra in each chemical phase. Sit back and let AutoPiFM do the work!
Automatic alignment
An industry first! The critical alignment of the excitation laser is now performed using computer vision, ensuring optimal results, reducing training, and saving time.
Compact footprint
Because of our automated beam alignment and integrated multiplexer, we can package the lasers below the main instrument. This creates a more compact design without compromises. Vista 300 supports up to two lasers to cover the full IR spectral range (see specifications).
Controlled environment
Maximise efficiency, minimise disruption
The 400 mm wide sample access door allows you to maximise throughput while minimising thermal disturbances that can cause drift. The insulated metal enclosure ensures acoustic isolation and stable temperature control within 0.1 °C, while also being clean room compatible.
Specifications
Stage and scanner
Sample stage travel: 300 mm × 300 mm square.
Scan size: 90 µm × 90 µm.
Dual Z Feedback: 12 µm z-scanner with 600 nm fast-z scanner provides both high bandwidth and a large z-range
Functionality
Imaging modes: Non-contact AFM, PiFM, KPFM, cAFM, nano DMA, FvD (force vs distance) mapping.
Spectroscopy modes: PiF-IR, FvD.
PiF Laser Options: QCL (770 – 1840, 1995 – 2395 cm−1), OPO/DFG (590 – 2050, 2250 – 4400, 5000 – 7000 cm−1).
Depth probed (IR): 20 nm in surface mode & greater than 100 nm in bulk mode.
Physical requirements
System dimensions: Approximately 1.1 m × 1.1 m × 4.9 m (3’ 7.3” × 3’ 7.3”× 5”)
Enclosure: 400 mm × 200 mm access door minimizes thermal drift. The enclosure is removable without disconnecting cables.
VIDEOS
Downloads
Supplier Info
APPLICATIONS
Reveal Hidden Structure in Colour
PiFM images are infrared absorption maps which can be used to locate materials. In this example, an EUV photoresist has been exposed with a low dose. The surface is scanned with PiFM before the resist is developed, so the latent image in the photoresist does not appear in the topography. However, two combined PiFM chemical maps can reveal the 16 nm half-pitch structure. Once the resist is developed, the final product can be verified with SEM imaging. Scan dimensions: 300 nm × 600 nm × 2.1 nm.
Sub-5 nm IR spatial resolution
A DNA origami molecule on a silicon substrate. The line trace plots the intensity of the data in the PiFM image (as opposed to the cross section of the topographic height). The steep rise in absorption intensity at the edge of the molecule shows a spatial resolution of less than 5 nm in the infrared imaging capabilities of Vista 300. Scan dimensions: 200 nm × 200 nm × 3.8 nm.
Single-molecule-level sensitivity
Aminosilane monolayers are a popular for surface functionalization. Conventional wisdom is that the aminosilane will form a uniform monolayer on a clean glass substrate. However, when analyzing some of these functionalized surfaces with PiFM, a different story appears. Instead, it seems that the aminosilane has formed small clusters that are distributed across the surface. The smallest cluster in this image is only 0.65 nm tall! The spectra show that the intensity of the aminosilane peak at 1677 cm−1 grows as the clusters get thicker. Similarly, the intensity of the substrate’s peak at 1060 cm−1 shrinks as that material is hidden under thicker clusters of aminosilane. Scan dimensions: 600 nm × 300 nm × 4.3 nm.
Defect analysis
This is a reference sample with different types of nanoparticles. Each of the PiF-IR spectra taken at the markers on the AFM topography image correlate very well with FTIR reference spectra allowing one to identify the materials as polystyrene (PS), polymethyl methacrylate (PMMA), and polytetrafluoroethylene (PTFE). With nanoparticles ranging in size from about 40 nm up to about 200 nm, this demonstrates how PiFM and PiF-IR can work together for nano defect analysis. Scan dimensions: 2 µm × 2 µm × 280 nm